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Science
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| Number of pages / Number of words: |
6 / 1526 |
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Reflux continued for a total of 60 minutes after the reflux ring formed and took approximately ten minutes to cool down to room temperature. Then the room temperature mixture was prepared for extraction with 10mL of water but discovered to be still very acidic after one wash. To reach a neutral pH, it took three washes with Sodium Bicarbonate (NaHCO3) to remove any excess acetic acid and catalytic sulfuric acid...
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To reach a neutral pH, it took three washes with Sodium Bicarbonate (NaHCO3) to remove any excess acetic acid and catalytic sulfuric acid. During distillation, the first drop was observed at 135 C and stopped at approximately 139 C when the distilling flask approached dryness. The final product was clear and colorless with a strong scent of bananas...
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