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The extraction with the soda can then be performed after the water has been removed.) Carefully run off the heavy lower layer of chloroform into a small conical flask, dry it over calcium chloride for 15-20 minutes, and then filter it directly into a 75 ml. distilling-flask fitted with a clean dry water-condenser...
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distilling-flask fitted with a clean dry water-condenser. Distill the chloroform, collecting the fraction of bp. 60-63oC. Yield, 30g. (20ml).
Chloroform is a colourless liquid, of bp 61o and d 1.50. It has a characteristic sweetish smell, and is frequently used as a solvent in organic chemistry.
Reference: Mann & Saunders, Practical Organic Chemistry, 3rd Ed
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Chloroform from Sodium Hypochlorite and Acetone
by Cheapskate
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Go get a five gallon bucket...
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