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| Topic: |
Science
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| Number of pages / Number of words: |
4 / 944 |
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The melting point is close to the literature Mp, and also has a narrow range which is indicative of minimal impurities. The product was also recrystallized using a minimum amount of boiling water as the recrystallization solvent, since the product was soluble in boiling water but insoluble in room temperature water...
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This gave an 83.53% recovery yield and a melting point of 144-146°C, which is a bit high and indicates the presence of impurities. .
Post Lab Questions:
1. The amide synthesis gave a crude product yield of 200.15%. This was due to the fact that acid may have been left in the product and was never sufficiently washed out...
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