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Science
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| Number of pages / Number of words: |
4 / 868 |
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After refluxing for the allotted time the distillate was poured while hot, to maximize the amount of adduct transferred, into an Erlenmyer flask and allowed to cool to room temperature before placing it an ice bath (We don't Want Broken Glass and Product contaminating our ice bath!). While hot, the solvent keeps the solute dissolved, in a easily transferable liquid state, but loses it solvating ability at cooler temperatures, thus the adduct crystallizes...
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After its ice bath the solution needs to be suction filtered to separate it from the xylenes (solvent). With the apparatus setup, hose connected and filter paper wet with solvent and aspirator running, the solution can be poured semi-slowly into the buchner funnel. The crystals tend to cling to the bottom and sides of the flask so a spatula will probably be needed to scrape them out...
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