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| Topic: |
Science
|
| Number of pages / Number of words: |
4 / 922 |
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When the ice was completely melted, the crude sample was isolated by vacuum filtration. The crude sample was purified by recrystallization using methanol as the solvent. The sample was packed inside the capillary tube and the Thiele Tube melting point set-up was prepared. Melting point was then obtained...
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Melting point was then obtained. The TLC profile of the sample was also obtained. The sample was spotted in a TLC plate and it was placed inside a beaker with a solvent. When the solvent totally reach the peak of the TLC plate, it was then placed in a beaker with iodine crystals. The TLC plate was inspected under UV light to see the distance travelled by the component and the developing medium...
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