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Addition of sodium chloride aided in suppressing
the solubility of the ketone, allowing for separation. To purify the
cyclohexanone, simple distillation was used collecting the distillate
within a five point boiling range of that listed in the Merck Index.
An Infrared Spectrum of the recovered material on the
Perkin-Elmer Spectrum RXI FT-IR will aid in the determination of the
composition of the recovered material...
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The
Infrared Spectrum of the sample follows on page 4.
Conclusion
The Infrared spectrum for cyclohexanone below, from McMurry's
"Organic Chemistry" has two distinctive absorption's relevant in this
experiment, the aliphatic C-H stretch around 2900 cm-1 and the C=O
stretch around 1750 cm-1.
The Infrared spectrum for adipic acid below, from McMurry's
"Organic Chemistry" also has two distinctive absorption's relevant in
this experiment, the C=O stretch around 1750 cm-1 and the O-H
stretch around 3000 cm-1...
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